Qualitative Pharmaceutical Chemistry 
                                                                              
                                          
                                          
                         Practical Book 
                         2019 
                                                                                                              Masfria                                                           
                         
                                                                                                              Muchlisyam                                                   
                                                                                                              Tuty Roida Pardede                                     
                         
                                                                                                              Yade Metri Permata 
                         
                         
                         
                         
                         
                         
                         
                         
                         
                         
                         
                        Qualitative Pharmaceutical Chemistry 
                        Laboratory               
                        Faculty of Pharmacy   
                        Universitas Sumatera Utara 
                                                                                                          
                            Qualitative  
                   Pharmaceutical Chemistry  
                            Laboratory 
                                  
                                           
                                  
                                  
                   YADE METRI PERMATA, S.Farm., M.Si., Apt. 
                        Prof.Dr. MASFRIA, M.S., Apt. 
                      Prof.Dr. MUCHLISYAM, M.Si., Apt. 
                    Dra. TUTY ROIDA PARDEDE, M.Si., Apt. 
                                  
                                  
                                  
                    Qualitative Pharmaceutical Chemistry Laboratory 
                            Faculty of Pharmacy 
                          University of Sumatera Utara 
                                Medan 
                                2019 
                                  
                                Preface 
             
            This book is arranged to complement the knowledge about the identification of the 
            various drug and chemical compounds quickly by chemical reaction in accordance 
            with our experience in laboratory Qualitative Pharmaceutical Chemistry. This book 
            can be used as a guide for students as teaching material in Chemistry Analysis. This 
            book was made on the awareness that the conventional chemical identification of 
            medicines still needed, although there is so many progress of modern technology of 
            qualitative  identification.  If  using  identification  technology  with  modern  and 
            sophisticated  tools  require  huge  costs  and  a  long  time.  It  is  our  experience  when 
            receiving multiple requests to identify some unknown material, but the identification 
            by  using  some  chemical  reaction  and  in  a  short  time  has  been  able  to  know  the 
            content of the material. 
             
             
             
                                  
            

            

            

            

            

            

            

            

            

            

            

            

            

            

            

            

            

            

            

            

            

            


	
	
	











            



	


	




	 
                                 2 
             
                                                                      CONTENTS 
                             
                            Preface 
                            Contents 
                            Experiment 1   Dry Analysis (flame test, sublimation, pyrolysis) 
                                                                       +    +2    +2   +3    +2    +2    +3    +2   +3
                            Experiment 2   Analysis of Cation (Ag ,Pb ,Hg ,Bi ,Cd ,Cu ,As ,Fe ,Fe ) 
                                                                       +3    +2     +2    +2     +2   +     +      +
                            Experiment 3   Analysis of Cation (Al , Zn , Ca , Ba , Mg ,K , Na , NH4 ) 
                                                                      -    -  -      -      -     3-     -
                            Experiment 4   Analysis of Anion (Cl , Br , I , NO , NO , PO             ClO)           
                                                                                    2      3     4
                                                                        2-     2-     2-      -2        -
                            Experiment 5   Analysis of Anion (SO         ,SO ,S O , CO , HCO ,borat, tetraborat) 
                                                                       4      3    2 3       3         3
                            Experiment 6   Practical Test of Cation and Anion 
                            Experiment 7   Functional Group dan Infra red Analysis 
                            Experiment 8   C,H,O Compound Analysis 
                            Experiment 9   C,H,O,N Compound Analysis Part I 
                            Experiment 10 C,H,O,N Compound Analysis Part II 
                            Experiment 11 C,H,O,N,S Compound Analysis 
                            Experiment 12 Practical Test 
                                                                            3